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光谱实验室

紫外可见近红外分光光度计 UV-VIS-NIR Spectrophotometer (SHIMADZU UV-3600 Plus)

仪器编号:

联系人:程园

联系方式:18800270665

地址:西湖大学(云谷校区)E10-144

开放范围:自主操作:校内;委托测试:校内、校外 Independent-operation :Internal ; Commissioned Service :Internal/External

  • 仪器编号 LHA19040019 规格
    生产厂家 岛津 型号 UV-3600Plus
    制造国家
    分类号 010401
    放置地点 云栖校区 4号楼219-220 出厂日期
    购置日期 2019/03/05 入网时间 2019/06/25
    主要规格及技术指标 测定波长范围: 185~3300nm
    波长准确性: 紫外、可见区:±0.2nm 近红外区:±0.8nm
    波长重复精度: 紫外、可见区:±0.08nm以内 近红外区:±0.32nm以内
    波长扫描速度: 波长移动速度:紫外、可见区:约18000nm/min 近红外区:约70000nm/min; 波长扫描速度: 紫外、可见区:约4500nm/min 近红外PMT/InGaAs区:约9000nm/min 近红外PbS区:约4000nm/min (各种切换所需时间除外)
    波长采样间隔: 0.01~5nm
    光源切换波长: 和波长同步自动切换282.0 nm~393.0 nm(0.1nm单位)
    谱带宽度: 紫外、可见区:0.1/ 0.2/ 0.5/ 1/ 2/ 3/5/8nm 8档转换
    近红外区: 0.2/ 0.5/ 1/ 2/ 3/5/8/12/20/32nm 10档转换
    分辨率: 0.1nm
    杂散光: 0.00008% 以下 (220nm,Nal )
    0.00005% 以下 (340nm, NaNO2)
    0.0005% 以下 (1420nm, H2O)
    0.005% 以下 (2365nm, CHCl3) "
    测光方式: 双光束测光方式
    测光类型: 吸光度(Abs),透射率(%),反射率,能量(E)
    测光范围: 吸光度:-6~6 Abs
    光度准确性:±0.003Abs(1Abs) ±0.002Abs(0.5Abs)
    以上由NIST930D标准滤光镜测试"
    光度重复精度:±0.0008Abs.(0~0.5Abs),±0.0016Abs(0.5~1.0Abs) 1秒计算,
    5次测定的最大偏差
    噪音 0.00005Abs RMS (500nm)
    0.00008Abs 以下 (900nm)
    0.00003Abs 以下 (1500nm) 狭缝2nm,1秒响应时的RMS值
    基线平直度 ±0.004Abs(185-200nm)
    ±0.001Abs(200-3000nm)
    ±0.005Abs(3000-3300nm)
    漂移:小于0.0002Abs/h (电源启动2小时后,500nm,1秒积算)
    基线校正:计算机自动校正(电源启动时,自动存储备份的基线,可以再校正)
    光源: 50W卤素灯和氘灯(插座型)
    检测器 紫外、可见区:光电倍增管PMT R-928
    近红外区:InGaAs光电二极管和冷却型PbS光电导原件

    主要功能及特色 波长测试范围至3300nm,配有积分球附件,可用于固体和薄膜的吸收、透射和反射测试。广泛应用于无机金属离子分析、有机化合物分析、有机化合物定性定量分析、有机化合物的结构解析,在化学研究中,可用于各类平衡常数、解离常数的测定
    主要附件及配置 *积分球:波长范围:220-2600nm, 60mm内径,标配PMT/InGaAs/PbS三检测器
    薄膜支架:用于较薄样品的透射测定,如薄膜和滤光片。样品尺寸:最小 W 16 × H 32 mm,最大 W 80 × H 40 × D 20 mm
    旋转膜支架:该薄膜支架可以使样品(以光轴为中心)在平面上旋转。偏光镜I、 II和III可以使用。测量样品尺寸:W 33 × H 30 × D 2 mm
    镜面反射装置 (5°入射角):该附件用于相对镜面反射率测试。最大样品尺寸为W 140 × H 160 × D 10 mm,最小样品直径为7mm。
    带光阑微量池支架:用于10mm长,4mm宽以下的半微量和微量池,光阑宽可连续调整
    微小样品支架(用于60mm积分球):用于放置5-10mm方形或者圆形,厚度为1-5mm的样品。样品通过上下方的夹子进行固定

     

  • 技术资料:https://iscps.westlake.edu.cn/info/1131/1302.htm


    送样要求:液体,粉末,薄膜,晶片,玻璃等。样品尺寸参照仪器详细参数

  • 类型

    项目

    细则

    校内

    校外

    说明

    自主上机

    自主操作

    液体、固体、常温、变温全波段测试

    80/

    160元/小时

    /

    委托测试

    光谱/光度测试

    液体、固体、常温、变温全波段测试

    120/小时

    2000/小时

    测试时间≤30   min,若超过则按50/30min收费

    培训

    仪器培训

    一对一/一对二培训;同等内容的第二次培训,收费1.5

    120/

    200元/小时


  • Instrument No.          LHA19040019                                                          Specification

    Manufacture              Shimadzu                                                                 Model                          UV-3600 Plus

    Made in                     Japan                                                                       Classification No.

    Location                    4#220                                                                       Manufacture date

    Purchase Date           5/03/2019                                                                 Internet access time     25/06/2019

    Main Technical specifications

    Wavelength range: 185~3300nm

    Wavelength accuracy: UVVIS±0.2nm NIR±0.8nm

    Wavelength repeatability: UVVIS±0.08nm  NIR±0.32nm

    Wavelength scanning speed:

    1. Wavelength moving speed : UVVISabout 18000nm/min  NIRabout 70000nm/min

    2. Wavelength scanning speed: UVVISabout 4500nm/min  NIR-PMT/InGaAsabout 9000nm/min NIR-PbSabout 4000nm/min

    Wavelength sampling interval: 0.015nm

    Light switching wavelength: synchronization automatically switch 282.0 nm~393.0 nm0.1nm unit

    Band width: UVVIS0.1/ 0.2/ 0.5/ 1/ 2/ 3/5/8nm  8 grade switch

    NIR 0.2/ 0.5/ 1/ 2/ 3/5/8/12/20/32nm 10 grade switch

    Resolution: 0.1nm

    Stray light: below 0.00008% (220nm,Nal )

    0.00005% below (340nm, NaNO2)

    0.0005% below (1420nm, H2O)

    0.005% below (2365nm, CHCl3) "

    Measurement mode: Dual beam system

    Measurement type: AbsorbanceAbs),T(%),ReflectivityEnergyE

    Absorbance Range :-6~6 Abs

    Photometric accuracy±0.003Abs(1Abs) ±0.002Abs(0.5Abs)

    Above tested by NIST930D standard filter"

    Photometric repeatability±0.0008Abs.(00.5Abs)±0.0016Abs(0.51.0Abs)

    Maximum deviation of 5 measurements

    Noise 0.00005Abs RMS (500nm)

    0.00008Abs below (900nm)

    0.00003Abs below (1500nm) slit 2nmRMS value at 1 second response

    Baseline flatness ±0.004Abs185-200nm

    ±0.001Abs200-3000nm

    ±0.005Abs3000-3300nm

    Driftingless than 0.0002Abs/h (Power on for 2 hours, 500nm, 1 second)

    Baseline correction: automatic correction by computer

    Light source: 50W halogen lamp and deuterium lamp (socket type)

    Detector UV/VIS PMT R-928

    NIRInGaAs photodiode and cooled PbS photoconductive elements



    Main functions and features


    The measurement range is up to 3300 nm, equipped with integrating sphere accessory for solid and thin film absorbance, transmission and reflection testing. It’s widely used in inorganic metal ion analysis, organic compound analysis, organic compound qualitative and quantitative analysis, organic compound structure analysis, and various equilibrium constants, dissociation constants

     

    Accessories and configuration


    1. Integrating sphere: wavelength range: 220-2600nm, 60mm inner diameter, PMT/InGaAs/PbS detector

    2. Film holder: used for transmission measurement of thinner samples, such as film and filter. Sample size: minimum W 16 × H 32 mm, maximum W 80 × H 40 × D 20 mm

    3. Rotating film holder: this film holder enables the sample (centered on the optical axis) to rotate on a plane. Polarizer I, II and III are available. Measurement sample size: W 33 × H 30 × D 2 mm

    4. Specular reflector (5° incident angle): this attachment is used for relative specular reflectance testing. The maximum sample size is W 140 × H 160 × D 10 mm, and the minimum sample diameter is 7mm.

    5. Micro sample holder with aperture: semi-micro and micro cuvette up to 10mm long and 4mm wide, aperture width can be adjusted continuously

    6. Micro sample holder (for 60mm integrating sphere) : for placing 5-10mm square or round samples with thickness of 1-5mm.The sample is fixed through clamps at the top and bottom.

     

  • Informations: https://iscps.westlake.edu.cn/info/1131/1302.htm

    Sample requirements: liquid, powder, film, wafer, glass, etc. The sample size refer to the part of instrument details

     


  • Operation Types

    Items

    Requirements

    Internal prices

    External prices

    Comments

    Independent   operation

    Liquid, solid, RT, vary-temperature   measurement in Full wavelength

    After being well-trained and authorized,   Make an appointment online

    ¥80/hour

    ¥160/hour

    /

    Commissioned   test

    Spectrum   Photometric measurement

    Liquid, solid, RT, vary-temperature   measurement in Full wavelength

    ¥120/hour

    ¥200/hour

    If   testing time exceed 30min, the extra time will be charged as ¥50/30min

    Training

    Instrument   training

    One-on-one   or one-on-two training. The first training session is normal charge. Any   subsequent training for the same instrument will be charged as a rate of 1.5 times.  

    ¥120/hour

    200元/hour